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[Determination of Si, Al and other in biological samples by ICP-AES with fusion with LiBO2 after dry ashing].

Identifieur interne : 003746 ( Main/Exploration ); précédent : 003745; suivant : 003747

[Determination of Si, Al and other in biological samples by ICP-AES with fusion with LiBO2 after dry ashing].

Auteurs : De-Zhong Sun [République populaire de Chine] ; Hong-Liao He ; Hong-Li Wen ; Sheng-Feng Ma ; Ai-Hua Gong ; Shao-Quan Yin

Source :

RBID : pubmed:18422151

Descripteurs français

English descriptors

Abstract

An alkaline sample digestion procedure using fusion with lithium metaborate (LiBO2) after dry ashing was developed. Silicon, aluminium and other, a total of 10 elements in different kinds of biological samples, were measured by ICP-AES. The detection limit of this method was 0.15 microg x mL(-1) for Si and 0.03 microg x mL(-1) for Al. The accuracy and precision of the method were demonstrated by analyzing certified reference materials poplar leaves (GBW07604). The precision was less than 3% and the accuracy was -0.03% for Si and -3% for Al. This method was applied to the certification of a series of ten biological reference materials. The results were satisfied.

PubMed: 18422151


Affiliations:


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Le document en format XML

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<title xml:lang="en">[Determination of Si, Al and other in biological samples by ICP-AES with fusion with LiBO2 after dry ashing].</title>
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<name sortKey="He, Hong Liao" sort="He, Hong Liao" uniqKey="He H" first="Hong-Liao" last="He">Hong-Liao He</name>
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<name sortKey="Wen, Hong Li" sort="Wen, Hong Li" uniqKey="Wen H" first="Hong-Li" last="Wen">Hong-Li Wen</name>
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<name sortKey="Ma, Sheng Feng" sort="Ma, Sheng Feng" uniqKey="Ma S" first="Sheng-Feng" last="Ma">Sheng-Feng Ma</name>
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<name sortKey="Gong, Ai Hua" sort="Gong, Ai Hua" uniqKey="Gong A" first="Ai-Hua" last="Gong">Ai-Hua Gong</name>
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<term>Aluminum (analysis)</term>
<term>Aluminum (chemistry)</term>
<term>Borates (chemistry)</term>
<term>Food Analysis (MeSH)</term>
<term>Limit of Detection (MeSH)</term>
<term>Lithium (chemistry)</term>
<term>Organosilicon Compounds (chemistry)</term>
<term>Plants (chemistry)</term>
<term>Reference Standards (MeSH)</term>
<term>Silicon (analysis)</term>
<term>Silicon (chemistry)</term>
<term>Solvents (chemistry)</term>
<term>Spectrophotometry, Atomic (standards)</term>
<term>Temperature (MeSH)</term>
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<term>Aluminium (analyse)</term>
<term>Aluminium (composition chimique)</term>
<term>Analyse d'aliment (MeSH)</term>
<term>Borates (composition chimique)</term>
<term>Composés organiques du silicium (composition chimique)</term>
<term>Limite de détection (MeSH)</term>
<term>Lithium (composition chimique)</term>
<term>Normes de référence (MeSH)</term>
<term>Plantes (composition chimique)</term>
<term>Silicium (analyse)</term>
<term>Silicium (composition chimique)</term>
<term>Solvants (composition chimique)</term>
<term>Spectrophotométrie atomique (normes)</term>
<term>Température (MeSH)</term>
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<term>Aluminum</term>
<term>Silicon</term>
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<term>Aluminum</term>
<term>Borates</term>
<term>Lithium</term>
<term>Organosilicon Compounds</term>
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<term>Solvents</term>
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<term>Borates</term>
<term>Composés organiques du silicium</term>
<term>Lithium</term>
<term>Plantes</term>
<term>Silicium</term>
<term>Solvants</term>
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<term>Limit of Detection</term>
<term>Reference Standards</term>
<term>Temperature</term>
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<front>
<div type="abstract" xml:lang="en">An alkaline sample digestion procedure using fusion with lithium metaborate (LiBO2) after dry ashing was developed. Silicon, aluminium and other, a total of 10 elements in different kinds of biological samples, were measured by ICP-AES. The detection limit of this method was 0.15 microg x mL(-1) for Si and 0.03 microg x mL(-1) for Al. The accuracy and precision of the method were demonstrated by analyzing certified reference materials poplar leaves (GBW07604). The precision was less than 3% and the accuracy was -0.03% for Si and -3% for Al. This method was applied to the certification of a series of ten biological reference materials. The results were satisfied.</div>
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<AbstractText>An alkaline sample digestion procedure using fusion with lithium metaborate (LiBO2) after dry ashing was developed. Silicon, aluminium and other, a total of 10 elements in different kinds of biological samples, were measured by ICP-AES. The detection limit of this method was 0.15 microg x mL(-1) for Si and 0.03 microg x mL(-1) for Al. The accuracy and precision of the method were demonstrated by analyzing certified reference materials poplar leaves (GBW07604). The precision was less than 3% and the accuracy was -0.03% for Si and -3% for Al. This method was applied to the certification of a series of ten biological reference materials. The results were satisfied.</AbstractText>
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